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3D microstructure evaluation of developed Si3N4 material for alloyed wire rolling applications
Lövy, Vít ; Salamon, David (referee) ; Chlup, Zdeněk (advisor)
This diploma thesis is devoted to the use of 3D reconstruction using EBSD method for microstructural analysis of silicon nitride ceramic material predetermined for the rolling-mill used in the wire production. Application of this method can be used for the grain structure reconstruction and basic microstructural parameters can be than extracted. The development of a suitable method for 3D reconstruction of the structure of the materials the main aim of this work. There are described the different steps begun by sample preparation from the investigated material trough the optimisation of analysis parameters up to the visualization of the grain structure. New type of sample geometry has been designed which leads to the better and faster observation of the microstructure of ceramic materials. This thesis also describes optimal reconstruction parameters such as the geometry of the assembly used in the microscope without mechanical movement of the sample or the influence of conductive coating prepared via in-situ sputtering of suitable metal, or adjustment of the electron and ion beams. Further are described two options of software which can be used for the final generation of 3D structure information and are assessed their advantages and disadvantages. The effect of the filter setting and other parameters and their influence on the resulting structural parameters are also evaluated.
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Structural analysis of austenitic weld joints
Procházka, Robert ; Foret, Rudolf (referee) ; Havlík, Petr (advisor)
The bachelor thesis deals with structural analysis of austenitic weld joints by using methods of material science. The theoretical part of the thesis summarizes the problematics of welding of high-alloy steels. After the general definition of welding and weldability of high-alloy steels, the thesis focuses on structural adjustments including welding defects during the welding process. Selected methods of fusion welding that were used to create these welds are mentioned in the second half of the theoretical part. The experimental part covers the structural analysis of the welds, which consists of microstructure evaluation, chemical composition analysis, and microhardness test.
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Immiscible alloy based on Fe-Cu system
Semerák, Petr ; Havlík, Petr (referee) ; Jan, Vít (advisor)
The aim of this work is the preparation of FeCuMn alloy in equimolar composition by melting and the analysis of the resulting microstructure. The theoretical part of the work deals with miscibility and the use of immiscible systems in practical applications. Furthermore, the influence of cooling rate and the effect of the ratio of the components of the immiscible Fe-Cu system on the resulting microstructure are described. The practical part of the work presents the microstructure of FeCuMn alloy, which was prepared by melting in an induction furnace under a protective atmosphere of argon. Furthermore, the practical part deals with the chemical composition of the individual phases and the shape of the resulting phases. For the FeCuMn alloy, the melting temperature of the phases is analysed, the material is also deformed, and the hardness of the deformed and undeformed material is evaluated. In the subsequent discussion, the results from the experimental part are related to published experimental results by other authors.
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Welding technology of turbine rotors
Pivoňka, Vít ; Kubíček, Jaroslav (referee) ; Daněk, Ladislav (advisor)
The paper deals with all the possibilities which can be used to weld the rotors of turbines, both the root and the filler welding. All these methods are thoroughly analyzed and their properties are described, especially the size of the heat input by welding of rotors of turbines. Further in this work is described the organization of the structure by means of a metallographic survey and a test of welds and materials, which are performed to check whether the material and the welding method are suitable for welding of rotors of turbines. In the experimental part are described all welds made by different welding parameters, one of these welds is chosen to achieve the best welding of the weld root. This weld is further investigated for hardness and change of microstructure after welding.
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Influence of the electron beam trajectory on the surface properties of steel 42CrMo4
Mikuš, Tomáš ; Kouřil, Miloslav (referee) ; Foret, Rudolf (advisor)
The thesis deals with surface quenching of steel 42CrMo4 by electron beam. Influence of technologic parameters and beam deflection on properties and structure of prepared layers is studied. Electron beam surface quenching was applicated with and without melting of the surface. Structures of layers made by electron beam quenching were compared with structures made by laser and electromagnetic induction. Structures and phases were analysed by optical microscopy, SEM and roentgen diffraction. Hardness was measured on hardened layers.
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Physical Phenomenon as a Creative Method in Architecture
Buryová, Tereza ; Mach, Jan (referee) ; Kristek,, Jan (advisor)
Cellular_ polar research station Antarctica is the driest, the busiest and most extensive place on Earth, half-year-shrouded. People still live here. They set up the research stations in which they live and work. In these extreme climatic conditions, the station originates and disappears due to natural behaving. Stations provide researchers with safety and space for research, including comfort. They are built in different ways and provide different comforts, according to technological and transport options.
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Fracture behaviour of heat affected zone near heterogeneous weld joint
Jelínek, Vladimír ; Válka, Libor (referee) ; Juliš, Martin (advisor)
The study deals with mechanical characteristic of heterogeneous weld joint. The low carbon steel 22K and austenitic steel have been used as a experimetnal materials. The low carbon steel has special properties in basic condition. The sample has been evaluated in basic condition and after annealation. There have been evaluated impact of annealation proces to structure and mechanical charakteristics in experimental part of study. The particularised analysis of microstructure has been done by pictorial analysis. Mechanical characteristics has been examinated in both conditions by 2 different methods – measurment of microhardness according to Vickers and test of fracture toughness on compact tension specimens.
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Influence of thermal processing to microstructure of various steels
Kocman, Lukáš ; Havlík, Petr (referee) ; Štěpánek, Roman (advisor)
This bachelor thesis deals with the heat treatment of steel, especially measuring the influence of individual heat treatment technologies on changes in the microstructure of steels. The theoretical part of the work presents alloys of iron and carbon, furthermore describes their phase transformations in the solid state, particularly the transformation diagrams of steels. In another part of theoretical part, the basic heat treatment technologies and their influence on the mechanical properties and microstructure of steels are described. The experimental part deals with the preparation of metallographic samples and presents results of examining the microstructure and measuring the hardness of individual samples. At the end of the work the synthesis of the theoretical part and results of the experimental part is used for the partial and overall evaluation of the influence of heat treatment on the microstructure of steels.
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Effect of heat treatments on the microstructure and hardness of high-entropy alloy
Jesenská, Mária Ľudmila ; Adam, Ondřej (referee) ; Moravčíková de Almeida Gouvea, Larissa (advisor)
V tejto práci je študovaná neekviatomická Al0.2Co1.5CrFeNi1.5Ti vysoko entropická zliatina, ktorá bola vyrobená pomocou vákuového indukčného tavenia. Zliatina v odliatom stave bola analyzovaná a tepelne spracovaná pri teplote 1000 °C po dobu 5h, a následne podrobená tepelnému spracovaniu pri teplote 750 °C po dobu ďalších 5h, s cieľom skúmania vplyvu teploty a doby tepelného spracovania na fázové zloženie, mikroštruktúru a mechanické vlastnosti. Na vyhodnotenie možných fáz prítomných v zliatine bol použitý pseudobinárny fázový diagram (CALPHAD). Mikroštruktúra zliatin bola charakterizovaná a chemicky analyzovaná pomocou röntgenovej difrakcie (XRD), elektrónovej mikroskopie (SEM) a energeticky disperznej spektroskopie. Výsledné vyhodnotenie tvrdosti materiálu prebehlo pomocou skúšok mikrotvrdosti a nanoindentácie.
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Microstructure of high-alloy steels
Feller, Šimon ; Bořil, Petr (referee) ; Ostratický, Marek (advisor)
This bachelor thesis concerns formation of microstructure of high-alloy steels. In theoretic part there is summary of sorting high-alloy steels, possible structures and how these structures affect qualities of steel. For practical part two small experimental casts were created, which tried to imitate composition and structure of two another, much bigger casts. Microstructure, makrostructure and grain boundary segregation were compared.
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